Lithium-Ion Battery Fire Residues Analysis

EMSL Analytical, Inc. provides testing for lithium-ion battery fire residues in the Materials Science Laboratory. The major chemical components in lithium-ion batteries (LIB’s) are:

  • Lithium combined with a metal oxide (for cathode)
    • Lithium + Cobalt Oxide
    • Lithium + [Nickel + Cobalt+ Aluminum] Oxides
    • Lithium + [Nickel + Cobalt+ Manganese] Oxides
    • Lithium + [Nickel + Cobalt+ Manganese+ Aluminum] Oxides
  • Lithium + [Aluminum + Titanium] Phosphate (alternative for cathode)
  • Silicon-Carbon or Graphite (for anode)
  • Lithium Hexafluorophosphate LiPF6 (electrolyte)
  • Fluoropolymers (as binders)
  • Polymers (as separator)
AnalyteMethodSampling Guide and Additional Information
LiICP-MS
  • For air sample: 37 mm MCE cassette. 1-4 L/min, min 100 liters
  • Ghost Wipe or Invis-Wipe for surface sampling; 100 cm2 suggested.
  • Min 2 grams bulk residue.
Ni, Co, Mn, Al, Ti, PICP-MS
  • Ghost Wipe or Invis-Wipe for surface sampling; 100 cm2 suggested.
  • Min 2 grams bulk residue.
  • NIOSH 7300 for air (see current price book)
FluorideIC
  • Alcohol prep wipe for surface sampling; 100 cm2 suggested.
  • Min 2 grams bulk residue.
Hydrofluoric Acid/HFIC
  • NIOSH 7906; Area sampling only, not for personal monitoring

Note: It is suggested to start the lithium-ion battery fire residue investigation with lithium as target analyte because it is not a common element in the environment. For a more comprehensive investigation, analysis for additional metals and fluoride/HF should be added.

Contact John Passero jpassero@emsl.com for pricing.

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